Application of Monolithic Capillary Half Focusing X-Ray Lens in Micro-EXAFS Analytical Technology

SUN Tian-Xi; LIU Zhi-Guo; WEI Shi-Qiang; HE Bo; WEI Zheng; YANG Jun; ZENG Yi; LIN Xiao-Yan; CHU Xue-Lian; DING Xun-Liang

Chinese Physics C> 2007, Vol. 31> Issue(10) : 967-971

Application of Monolithic Capillary Half Focusing X-Ray Lens in Micro-EXAFS Analytical Technology

The Key Laboratory of Beam Technology and Materials Modification of Ministry of Education, Beijing Normal University,Institute of Low Energy Nuclear Physics, Beijing Normal University,Beijing Radiation Center,Beijing 100875,China2 National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230029, China

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Abstract：
A monolithic capillary half focusing X-ray lens (MCHFXRL) is used to focus the synchrotron radiation. The magnitudes of the focal spot size and gain of the synchrotron radiation microbeam focused by the MCHFXRL are in the orders of 10μm and 10³, respectively. In the energy range from 5.5 to 11.5keV, the focal spot size varies from 38 to 29μm; the transmission efficiency varies from 26.1% to 20.5%; the translation of the vertical position of the focal spot is 3μm; the change of the output focal distance is 155μm. On the basis of the investigation of the performances of the MCHFXRL, the application of the synchrotron radiation microbeam in micro-extended-X-ray-absorption-fine-structure (micro-EXAFS) analysis is studied.

References

[1]

. SUN Tian-Xi, DING Xun-Liang. J. Appl. Phys., 2005, 97:124904(-1)|124904(-7)2. SUN Tian-Xi, DING Xun-Liang. Nucl. Instrum. Methods,2004, B226: 651-6583. SUN Tian-Xi, DING Xun-Liang, LIU Zhi-Guo et al. ActaOptica Sinica, 2005, 25(10): 1436-1440(in Chinese)(孙天希，丁训良，刘志国,2005,25(10):1436—14404. DING Xun-Liang, HE Ye-Jun, YAN Yi-Ming. J. BeijingNormal University (Natural Science), 1995, 31(Supp.):75-795. DING Xun-Liang, LIANG Wei, YAN Yi-Ming. J. Bei-jing Normal University (Natural Science), 1995, 31(Supp.):40-506. DING Xun-Liang, LIANG Wei, YAN Yi-Ming. Nucl. Tech-niques, 1996, 19: 164-169 (in Chinese(丁训良，梁炜，颜一鸣.核技术，1996, 19: 164-169)7. DING Xun-Liang, HE Ye-Jun, YAN Yi-Ming. X-Ray Spec-trom., 1997, 26: 374-3798. DING Xun-Liang, LIANG Wei, YAN Yi-Ming. J.Trace andMicroprobe Techniques, 1997, 15(4): 647-6529. DING Xun-Liang, HE Ye-Jun, XIE Jin-Dong et al. Pro-ceedings of Japan-China Joint Seminar on Atomic LevelCharacterization. 1998, 112-11710. DING Xun-Liang, XIE Jing-Dong, HE Ye-Jun et al. Ta-lanta, 2000, 53: 17-2211. DING X, GAO N, Havrilla G. SPIE 4144, 2000, 174-18212. DING Xun-Liang, LIU Zhi-Guo, YAN Yi-Ming et al. X-Ray Spectrom., 2004, 33: 67-7313. Bjeoumikhov A, Bjeoumikhova S, Langho N et al. Appl.Phys. Lett., 2005, 86: 144102-144102(-3)14. Bartoll J, Rfhrs S, Erko A et al. Spectrochimica Acta Part,2004, B59: 1587-159215. Hofmann F A, Freinberg-Trufas C A, Owens S M et al.Nucl. Instrum. Methods, 1997, B133: 145-15016. Kuhbacher M, Weseloh G, Thomzig A et al. X-Ray Spec-trom., 2005, 34: 112-11717. Sirenko A A, Kazimirov A, HUANG R et al. J. Appl. Phys.,2005, 97: 063512-063512(-7)18. Vincze L, Somogyi A, Osan J et al. Anal. Chem., 2002, 74:1128-113519. Proost K, Vincze L, Janssens K et al. X-Ray Spectrom.,2003, 32: 215-22220. Rindby Anders, Engstrom Per, Janssens K et al. Nucl. In-strum. Methods, 1997, B124: 591-60421. Vincze L, Janssens K, Adams F et al. Rev. Sci. Instrum.,1998, 69(10): 3494-3503

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SUN Tian-Xi, LIU Zhi-Guo, WEI Shi-Qiang, HE Bo, WEI Zheng, YANG Jun, ZENG Yi, LIN Xiao-Yan, CHU Xue-Lian and DING Xun-Liang. Application of Monolithic Capillary Half Focusing X-Ray Lens in Micro-EXAFS Analytical Technology[J]. Chinese Physics C, 2007, 31(10): 967-971.

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Received: 2006-11-14
Revised: 2007-06-09

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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

Application of Monolithic Capillary Half Focusing X-Ray Lens in Micro-EXAFS Analytical Technology

Corresponding author: SUN Tian-Xi,

The Key Laboratory of Beam Technology and Materials Modification of Ministry of Education, Beijing Normal University,Institute of Low Energy Nuclear Physics, Beijing Normal University,Beijing Radiation Center,Beijing 100875,China2 National Synchrotron Radiation Laboratory, University of Science and Technology of China, Hefei 230029, China

Received Date: 2006-11-14

Accepted Date: 2007-06-09

Available Online: 2007-10-05

Abstract: A monolithic capillary half focusing X-ray lens (MCHFXRL) is used to focus the synchrotron radiation. The magnitudes of the focal spot size and gain of the synchrotron radiation microbeam focused by the MCHFXRL are in the orders of 10μm and 10³, respectively. In the energy range from 5.5 to 11.5keV, the focal spot size varies from 38 to 29μm; the transmission efficiency varies from 26.1% to 20.5%; the translation of the vertical position of the focal spot is 3μm; the change of the output focal distance is 155μm. On the basis of the investigation of the performances of the MCHFXRL, the application of the synchrotron radiation microbeam in micro-extended-X-ray-absorption-fine-structure (micro-EXAFS) analysis is studied.

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Application of Monolithic Capillary Half Focusing X-Ray Lens in Micro-EXAFS Analytical Technology

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